UIC Chemistry - NMR Facility

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Included here are some instructions for carrying out various operations on our spectrometers. These instructions are downloadable in Adobe PDF format. After downloading the file you can print it out or read it on your screen.

Since these instruction files are in Adobe PDF format, you will need Adobe Acrobat Reader installed on your computer to view the downloaded file.

If you need Acrobat Reader you can get it free from Adobe: .

General Rules and Regulations:
1) Basic guidelines for the use of the NMR Facility
2) Supplemental policy issues
3) Supplementary guidelines for the use of the Avance spectrometers
4) Sample preparation tips (HTML page - will open in a new window)

Bruker AV-500 (2210 SEL) Instructions (updated 02-2004):
1) Basic instruction and information packet for 1D experiments on the Bruker AV-500
2) Instruction packet for routine 2D experiments on the Bruker AV-500

Bruker Avance (RRC-East) Instructions (updated 07-2008):
1) Basic instruction and information packet for 1D experiments on the Bruker Avance
2) Instruction packet for routine 2D experiments on the Bruker Avance
3) Instruction packet for 19F NMR spectroscopy on the Bruker Avance with Bruker BBO probes
4) Hints and tips on 2D-NOESY spectroscopy on the Bruker Avance

5) 1D Selective NOE on DRX500

Bruker AM/AC (4130 SES) Instructions:
1) Basic instructions for 1H and 13C acquisition on our Bruker AM-400 and AC-200;
includes discussion of EP routine and phasing
2) 13C DEPT acquisition on our Bruker Spectrometers
3)* X-nucleus observation on our Bruker Spectrometers;

includes probe tuning procedures for Bruker Spectrometers with the Nalorac Broadband Probe

4)Transferring data from a Bruker Spectrometer to the PC

NOTE!! Procedures 1, 3, and 4 require that you be checked out by Facility Staff before performing the procedure by yourself.

Varian (2210 SEL) Instructions (updated 02-2005):

1) Basic 1D and 2D (COSY and HETCOR) experiments on the Varian

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